標(biāo)準(zhǔn)號：DIN EN ISO 22959-2009
中文標(biāo)準(zhǔn)名稱：動植物油脂.在線受體絡(luò)合物色譜法和熒光探測高效液相色譜法測定多環(huán)芳碳氫(ISO 22959:2009),德文版本EN ISO 22959:2009
英文標(biāo)準(zhǔn)名稱：Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection (ISO 22959:2009); English version of DIN EN ISO 22959:2009-10
標(biāo)準(zhǔn)類型：X14
發(fā)布日期：1999/12/31 12:00:00
實施日期：1999/12/31 12:00:00
中國標(biāo)準(zhǔn)分類號：X14
國際標(biāo)準(zhǔn)分類號：67.200.10
引用標(biāo)準(zhǔn)：ISO 661
適用范圍：This International Standard specifies a high performance liquid chromatographic (HPLC) procedure for thedetermination of polycyclic aromatic hydrocarbons (PAHs) in edible fats and oils.The method has been validated for coconut (CN), olive (OV), sunflower (SF), and soybean (BO) oil, and ispossibly applicable to other oils, dependent on the determination of appropriate parameters.The lowest level of quantification for the PAHs is 0,1 μg/kg. The lowest possible amount of each PAH whichcan be distinguished from the baseline noise has not been determined. The validated concentration range ofthe method is 0,1μg/kg to 3,5 IJg/kg for each individual PAH. For samples containing (light) PAH contents: 3,5 μg/kg, dilution to bring the contents into the validated range is possible. It is also possible to adjust therange of the calibration curves. However, ranges exceeding 3,5 μg/kg have not been validated.PAHs which can be determined by this method are: anthracene, phenanthrene, fluoranthene, pyrene,chrysene, benzo[a]anthracene, benzo[e]pyrene, benzo[a]pyrene, perylene, benzo[ghi]perylene, anthanthrene,dibenzo[a,h]anthracene, coronene, indeno[1,2,3-cd]pyrene, benzo[a]fluoranthene, benzo[b]fluoranthene,benzo[k]fluoranthene.